Method for Preparing WC-Co (tungsten carbide-cobalt) Nano-powder

The invention discloses a method for preparing WC-Co (tungsten carbide-cobalt) nano-powder, which comprises the following steps of: firstly, preparing tungsten oxide-cobalt oxide powder by adopting a citrate or package method; secondly, introducing ammonia gas into the obtained tungsten oxide-cobalt oxide powder for nitridation to obtain tungsten nitride-cobalt nitride powder; and thirdly, mixing the obtained tungsten nitride-cobalt nitride powder with carbon black, performing ball milling, and performing heat treatment under a vacuum or inert atmosphere with the air pressure of less than 200Pa to obtain the WC-Co nano-powder; or directly charging the obtained tungsten nitride-cobalt nitride powder into a tube furnace, and introducing mixed gas of methane and hydrogen gas into the tube furnace for carbonization to obtain the WC-Co nano-powder.

The preparation process disclosed by the invention has the advantages of simplicity and practicality, strong maneuverability, and easiness of large-scale production. Moreover, the prepared powder has the advantages of small particle diameter, uniform particle size distribution and good sintering activity.


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