Method and Apparatus for Preparing Blue Tungsten Oxide by Ammonium Paratungstate Self-reduction
- Details
- Category: Tungsten Patents
- Published on Monday, 01 December 2014 09:37
The present invention discloses a method and a device for the preparation of the self-reducible paratungstate blue tungsten oxide, ammonium paratungstate which is 5 (NH.
A method paratungstate since reducing preparation blue tungsten oxide, which is based paratungstate 5 (NH4) 2O · 12WO3 · 5H2O as raw material, characterized in that: it comprises the following steps:. A will paratungstate 5 (NH4) 2O · 12WO3 · 5H2O thermally decomposed into tungsten trioxide WO3, ammonia NH3 and water vapor H2O; paratungstate said heating temperature is 400 ℃ ~ 600 ℃;. b using the tungsten oxide WOX good properties of ammonia NH3 decomposition catalyst, and said control of the reaction; the heat decomposition of the ammonia NH3 is further decomposed into nitrogen N2 and hydrogen H2;. c by controlling the reaction temperature and the gas pressure of the furnace proper, the reduction of tungsten trioxide WO3 tungsten oxide blue WO2.9 temperature is set to 550 ℃ ~ 800 ℃; furnace gas pressure in the range of 0 to 2 mbar.
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