Contact Preparation of Tungsten Copper Contacts (Cu80W / Cu)

1. Selection of raw materials of tungsten copper contacts (Cu80W / Cu)
(1) Selection of tungsten powder. Select tungsten powder with the grade of FW-1 standard, tungsten powder particle size range is: 6-8μm. If the tungsten powder is oxidized, then the reduction of the oxidized tungsten powder is needed at the condition of hydrogen protection, and at a temperature of about 860 ℃, and holding 1h.
(2) Selection of copper powder. Adopting electrolytic copper method to obtain copper, which should be restored firstly, its reducing atmosphere is hydrogen atmosphere, temperature is about 300 ℃, holding time of 1h.

2. Preparation of contact 
Preparation of contact of tungsten copper contacts (Cu80W / Cu) adopts sintering and infiltration process of powder metallurgy.
Process:
Mixing powder (tungsten powder and copper powder, in accordance with an appropriate proportion) → pressing to its shape → sintering and infiltration (tungsten copper blanks) → machining and squeezing.
Sintering and infiltration conditions: the need for introducing hydrogen (hydrogen flow: 1m³ / h), the temperature is about 1500 ℃, sintering time is 2h.
Machining and squeezing: machining the tungsten copper blanks after sintering and infiltration, and then, coating its surface with oil evenly, then squeezing by using four-column hydraulic press machine.


Tungsten copper contacts

 

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A Primary Algorithm of Tungsten Ore Based on SUSAN Operator

Tungsten primary machine to achieve automatic sorting system is the key technology of tungsten ore image featureextraction,identification and sorting algorithm.SUSAN operator to improved fast algorithm as the core of tungsten ores and primary algorithm is a targeted optimum algorithm.A primary algorithm of tungsten ore based on SUSAN operator is designed and realized.The algorithm adopts the improved SUSAN edge extraction operator with morphological opening operation to estimate background and global gray image taking the original geometry of complex operations to weaken the background noise on the image texture and the influence.In order to improve the effect of edge detection,the algorithm is combined with the similarity SUSAN comparison based on image gray edge detection algorithm.The algorithm,which does not require gradient calculations,is simple,accurate in positioning and antinoise.The effect of edge detection is enhanced.

 

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Experiment Study of Tungsten Ore from Primary Slimes

The new type centrifugal separator was used to discarding the large number of tailings of tungsten ore from slims,and the next is that the gravity separation concentrate was put into the process of flotation.Of these mine samples,the degree of slimings is high and the particle size is very low,therefore the separation is very difficult.The experiment test through a flotation flowsheet of centrifugal-flotation was performed.The tungsten concentrate with the grade of 34.74 %WO3,and the total recovery of 75.21% can be obtained.

 

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Determination of Tungsten in Tungsten Ore by Spectrophotometry with Microwave Digestion

Microvave digestion method was applied in the determination of tungsten in tungsten ore by thiocyanate spectrophotometry.The digestion solvent was 40 mL of NaOH solution(25 g/L).The microwave power was medium-high level.The digestion time was 30 min.The dosages of all reagents were investigated.The detection limit of this method was 0.5 μg/mL.The tungsten ore was analyzed by the proposed method and the determination results were consistent with those obtained by the traditional sample preparation methods.The relative standard deviation(RSD) was less than 2.3 %.

 

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Potassium Tungstate

Potassium tungstate is white or colorless crystalline powder and is a monoclinic structure. Its physical properties are as follows: chemical formula: K2O4W, molecular weight: 326.0342, density: 3.12g/ml, melting point: 921 ℃, Solubility: soluble in water, insoluble in alcohol. K2O4W should be sealed in the storage vessel, and it is placed in a cool, dry place. Besides avoids contact with tungsten oxide, moisture or humidity. In addition, it is harm for the water, if there is no relevant government departments permission shouldn’t released to the surrounding.
Potassium tungstate is mainly used in analytical reagents, alkaloids precipitant, but also for the fine tungsten and bronze manufacture.
Potassium tungstate producing processes are as follows:
1.Mixed potassium dichromate (K2Cr2O7) with tungsten powder, after reaction to obtain potassium tungstate and chromium oxide.
2.W react with KOH to produce potassium tungstate.
W reacts with KOH solution, if no oxygen participate there is a slight reaction. But the reaction has oxidizing agent (such as KNO3, KNO2, KClO3, PbO2, etc.) will cause violet reaction.

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